%A K Mikami
%A H Matsuzawa
%A S Tekeuchi
%A Y Nakamura
%A DP Curran
%J Synlett
%T ?-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use ?-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis
%X Guidelines for the use of ?-cyclodextrin columns in fluorous and non-fluorous mixture synthesis, and racemic synthesis are suggested. Fluorous compounds can be separated more efficiently with SUMICHIRAL OA-7000 and -7100, while non-fluorous compounds can be separated better with SUMICHIRAL OA-7500. When the ratio of water in the mobile phase is large (>20%), the guard column (GL cart) can improve the separability of the fluorinated mixture.
%N 15
%P 2713 - 2716
%D 2004
%R 10.1055/s-2004-835649
%L pittir19861