%0 Journal Article
%@ 0936-5214
%A Mikami, K
%A Matsuzawa, H
%A Tekeuchi, S
%A Nakamura, Y
%A Curran, DP
%D 2004
%F pittir:19861
%J Synlett
%N 15
%P 2713 - 2716
%T β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis
%U http://d-scholarship-dev.library.pitt.edu/19861/
%X Guidelines for the use of β-cyclodextrin columns in fluorous and non-fluorous mixture synthesis, and racemic synthesis are suggested. Fluorous compounds can be separated more efficiently with SUMICHIRAL OA-7000 and -7100, while non-fluorous compounds can be separated better with SUMICHIRAL OA-7500. When the ratio of water in the mobile phase is large (>20%), the guard column (GL cart) can improve the separability of the fluorinated mixture.