Luo, Z and Swaleh, SM and Theil, F and Curran, DP
(2002)
Resolution of 1-(2-naphthyl)ethanol by a combination of an enzyme-catalyzed kinetic resolution with a fluorous triphasic separative reaction.
Organic Letters, 4 (15).
2585 - 2587.
ISSN 1523-7060
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Abstract
(Matrix presented) Kinetic resolution of a fluorous ester rac-1 with Candida antarctica B lipase provided a mixture of enantioenriched alcohol (R)-2 and fluorous ester (S)-1. The mixture was subjected to a fluorous triphasic reaction to give both enantiomers of 1-(2-naphthyl)ethanol 2 in high ee without chromatographic separation or fluorous-organic liquid-liquid extractive purification.
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Details
Item Type: |
Article
|
Status: |
Published |
Creators/Authors: |
Creators | Email | Pitt Username | ORCID |
---|
Luo, Z | | | | Swaleh, SM | | | | Theil, F | | | | Curran, DP | curran@pitt.edu | CURRAN | |
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Date: |
25 July 2002 |
Date Type: |
Publication |
Journal or Publication Title: |
Organic Letters |
Volume: |
4 |
Number: |
15 |
Page Range: |
2585 - 2587 |
DOI or Unique Handle: |
10.1021/ol026232f |
Schools and Programs: |
Dietrich School of Arts and Sciences > Chemistry |
Refereed: |
Yes |
ISSN: |
1523-7060 |
MeSH Headings: |
Catalysis; Esters--chemistry; Ethanol--analogs & derivatives; Ethanol--isolation & purification; Fluorescent Dyes; Fungal Proteins; Kinetics; Lipase--metabolism; Naphthalenes--isolation & purification; Solvents--chemistry; Stereoisomerism |
PubMed ID: |
12123382 |
Date Deposited: |
12 Feb 2014 23:43 |
Last Modified: |
02 Feb 2019 15:58 |
URI: |
http://d-scholarship-dev.library.pitt.edu/id/eprint/20490 |
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