Fluorous dienophiles are powerful diene scavengers in diels-alder reactions

Werner, S and Curran, DP (2003) Fluorous dienophiles are powerful diene scavengers in diels-alder reactions. Organic Letters, 5 (18). 3293 - 3296. ISSN 1523-7060

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Abstract

(Matrix presented) Three fluorous dienophiles have been synthesized, and their value in scavenging an excess diene after Diels-Alder reactions is shown. The resulting fluorous derivatives are separated by solid-phase extraction on fluorous silica gel (FSPE). The fluorous [1,2,4]triazoline-3,5-dione 10 reacted with most dienes within seconds or minutes.

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Details

Item Type:	Article
Status:	Published
Creators/Authors:	Creators Email Pitt Username ORCID Werner, S Curran, DP curran@pitt.edu CURRAN
Date:	4 September 2003
Date Type:	Publication
Journal or Publication Title:	Organic Letters
Volume:	5
Number:	18
Page Range:	3293 - 3296
DOI or Unique Handle:	10.1021/ol035214a
Schools and Programs:	Dietrich School of Arts and Sciences > Chemistry
Refereed:	Yes
ISSN:	1523-7060
MeSH Headings:	Aldehydes--chemistry; Alkenes--chemical synthesis; Amines--chemistry; Catalysis; Fluorine--chemistry; Maleimides--chemistry; Molecular Structure; Stereoisomerism; Triazoles--chemistry
PubMed ID:	12943410
Date Deposited:	30 Oct 2013 16:48
Last Modified:	02 Feb 2019 15:58
URI:	http://d-scholarship-dev.library.pitt.edu/id/eprint/19947

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