β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis

Mikami, K and Matsuzawa, H and Tekeuchi, S and Nakamura, Y and Curran, DP (2004) β-cyclodextrin columns for separation of fluorous and non-fluorous compounds: How to use β-cyclodextrin columns in fluorous mixture synthesis and racemic synthesis. Synlett (15). 2713 - 2716. ISSN 0936-5214

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Abstract

Guidelines for the use of β-cyclodextrin columns in fluorous and non-fluorous mixture synthesis, and racemic synthesis are suggested. Fluorous compounds can be separated more efficiently with SUMICHIRAL OA-7000 and -7100, while non-fluorous compounds can be separated better with SUMICHIRAL OA-7500. When the ratio of water in the mobile phase is large (>20%), the guard column (GL cart) can improve the separability of the fluorinated mixture.

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Details

Item Type:	Article
Status:	Published
Creators/Authors:	Creators Email Pitt Username ORCID Mikami, K Matsuzawa, H Tekeuchi, S Nakamura, Y Curran, DP curran@pitt.edu CURRAN
Date:	7 December 2004
Date Type:	Publication
Journal or Publication Title:	Synlett
Number:	15
Page Range:	2713 - 2716
DOI or Unique Handle:	10.1055/s-2004-835649
Schools and Programs:	Dietrich School of Arts and Sciences > Chemistry
Refereed:	Yes
ISSN:	0936-5214
Date Deposited:	09 Oct 2013 15:52
Last Modified:	02 Feb 2019 15:58
URI:	http://d-scholarship-dev.library.pitt.edu/id/eprint/19861

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