Purification of fluorous Mitsunobu reactions by liquid-liquid extraction

Curran, DP and Bajpai, R and Sanger, E (2006) Purification of fluorous Mitsunobu reactions by liquid-liquid extraction. Advanced Synthesis and Catalysis, 348 (12-13). 1621 - 1624. ISSN 1615-4150

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Abstract

Solvent tuning and partition coefficient measurements have identified suitable reagent and solvent combinations for the purification of fluorous Mitsunobu reaction products. The crude reaction mixtures are partitioned between 2/1 HFE-7100/FC-72 and DMF/10% water to provide reagent (fluorous) and product (organic) fractions. © 2006 Wiley-VCH Verlag GmbH & Co. KGaA.

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Details

Item Type:	Article
Status:	Published
Creators/Authors:	Creators Email Pitt Username ORCID Curran, DP curran@pitt.edu CURRAN Bajpai, R Sanger, E
Date:	1 August 2006
Date Type:	Publication
Journal or Publication Title:	Advanced Synthesis and Catalysis
Volume:	348
Number:	12-13
Page Range:	1621 - 1624
DOI or Unique Handle:	10.1002/adsc.200606187
Schools and Programs:	Dietrich School of Arts and Sciences > Chemistry
Refereed:	Yes
ISSN:	1615-4150
Date Deposited:	28 May 2013 14:51
Last Modified:	02 Feb 2019 15:58
URI:	http://d-scholarship-dev.library.pitt.edu/id/eprint/18742

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